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Custom Cryogenic Sample Holder

Research project · Wake Forest · Design, prototyping, machining and testing

A copper sample mount for a Montana Instruments cryostat that keeps samples aligned and cuts noise in low-temperature optical measurements.

~79%less noise at 20 K
~31%less noise at 300 K
< 5 nmpeak shift
Custom Cryogenic Sample Holder

The problem

Optical measurements in a cryostat need the sample to stay exactly in the beam while it cools. The old setup drifted, so the spectra were noisy.

The holder in the cryostat's optical path
The holder in the cryostat's optical path

The design

A 15-part copper assembly with a dovetail base, slider and wire holder that keeps the beam path clear and conducts heat well. I modeled it in Fusion 360 and Creo and checked fit with 3D prints.

Fusion 360 model of the holder
Fusion 360 model of the holder

Making it

I machined it in copper on a Tormach PCNC 440 with a Wazer waterjet. When the base hit the cryostat casing, I widened one mounting hole on the drill press to restore clearance.

Machining the copper part on the Tormach
Machining the copper part on the Tormach

Results

Noise dropped about 79% at 20 K and 31% at 300 K, and peaks shifted less than 5 nm, so the holder doesn't distort the measurement.

Installed in the cryostat
Installed in the cryostat